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Nanomedicines Analytical Development

Advanced analytical development for complex nanomedicine formulations

Overview

We are intimately familiar with defining the critical quality attributes (CQAs) of nanomedicines. To evaluate the CQAs of your GMP-produced drug products and to support product development, we utilize state-of-the-art analytical techniques.

We perform ICH-compliant stability testing of nanomedicines, APIs and novel excipients using stability indicating methods. Our expertise covers lipid nanoparticles, liposomes, and microspheres according to product-specific guidelines, with optimization of critical analytical processes and systematic approaches to address long-standing market complaints.

Analytical Techniques Used

Particle Analysis

  • Dynamic light scattering (DLS)
  • Small-angle X-ray scattering (SAXS)
  • Laser diffraction
  • Asymmetric flow field-flow fractionation (AF4-MALS)

Advanced Characterization

  • Capillary electrophoresis
  • Zeta-potential measurements
  • Size exclusion chromatography
  • Transmission and scanning electron microscopy

Spectroscopy & Molecular Analysis

Nuclear Magnetic Resonance

  • Solution-state NMR
  • Solid-state NMR
  • Diffusion-ordered spectroscopy

Vibrational Spectroscopy

  • Infrared spectroscopy (IR)
  • Raman spectroscopy
  • Surface-enhanced Raman spectroscopy (SERS)

Chromatography & Separation

HPLC/UPLC Analysis

  • Reverse-phase chromatography
  • Size exclusion chromatography
  • Ion exchange chromatography
  • Hydrophilic interaction chromatography

Detection Methods

  • UV-Vis detection
  • Mass spectrometry (MS)
  • Charged aerosol detection (CAD)
  • Refractive index detection (RI)

Critical Quality Attributes (CQAs)

Physical Properties

  • • Particle size distribution
  • • Morphology and shape
  • • Surface charge (zeta potential)
  • • Physical stability

Chemical Properties

  • • Drug loading and encapsulation
  • • Chemical stability
  • • Impurity profile
  • • Drug release kinetics

Biological Properties

  • • Biocompatibility
  • • Cellular uptake
  • • Biodistribution
  • • Therapeutic efficacy

ICH-Compliant Stability Testing

We perform comprehensive stability testing of nanomedicines, APIs and novel excipients using stability indicating methods. Our stability studies follow ICH guidelines and include:

Environmental Conditions

  • Temperature and humidity control
  • Light exposure testing
  • Accelerated stability studies

Analytical Monitoring

  • Physical appearance changes
  • Particle size stability
  • Drug content and impurities

Applications & Formulations

Lipid-Based Systems

  • Lipid nanoparticles (LNPs)
  • Liposomes and vesicles
  • Solid lipid nanoparticles

Polymer-Based Systems

  • Polymeric nanoparticles
  • Microspheres and nanospheres
  • Dendrimers and micelles

Ready to Develop Your Nanomedicine?

Contact our nanomedicines team to discuss your analytical development needs and CQA requirements.